Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR

In DNP MAS NMR experiments at ~80–110 K, the structurally important −(13)CH(3) and −(15)NH(3)(+) signals in MAS spectra of biological samples disappear due to the interference of the molecular motions with the (1)H decoupling. Here we investigate the effect of these dynamic processes on the NMR line...

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Udgivet i:J Phys Chem B
Main Authors: Ni, Qing Zhe, Markhasin, Evgeny, Can, Thach V., Corzilius, Björn, Tan, Kong Ooi, Barnes, Alexander B., Daviso, Eugenio, Su, Yongchao, Herzfeld, Judith, Griffin, Robert G.
Format: Artigo
Sprog:Inglês
Udgivet: 2017
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Article
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC5874497/
https://ncbi.nlm.nih.gov/pubmed/28437077
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.jpcb.7b02066
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