Synthesis, spectroscopic characterization and thermogravimetric analysis of two series of substituted (metallo)tetraphenylporphyrins

Subsequent treatment of H(2)TPP(CO(2)H)(4) (tetra(p-carboxylic acid phenyl)porphyrin, 1) with an excess of oxalyl chloride and HNR(2) afforded H(2)TPP(C(O)NR(2))(4) (R = Me, 2; iPr, 3) with yields exceeding 80%. The porphyrins 2 and 3 could be converted to the corresponding metalloporphyrins MTPP(C(...

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Publicat a:Beilstein J Nanotechnol
Autors principals: Al-Shewiki, Rasha K, Mende, Carola, Buschbeck, Roy, Siles, Pablo F, Schmidt, Oliver G, Rüffer, Tobias, Lang, Heinrich
Format: Artigo
Idioma:Inglês
Publicat: Beilstein-Institut 2017
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Full Research Paper
Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC5480337/
https://ncbi.nlm.nih.gov/pubmed/28685120
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjnano.8.121
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