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Study of Uridine 5′-Monophosphate (UDP)-Galactopyranose Mutase Using UDP-5-Fluoro-Galactopyranose As a Probe: Incubation Results and Mechanistic Implications
Uridine 5′-monophosphate-5-fluoro-galactopyranose (UDP-5F-Galp, 7) was synthesized and its effect on UDP-Galp mutase (UGM) was investigated. UGM facilitated the hydrolysis of 7 to yield UDP and 5-oxo-galactose (24), but no 11 was detected. (19)F-NMR and trapping experiments demonstrated that the rea...
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| Publicado no: | Org Lett |
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| Main Authors: | , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5474323/ https://ncbi.nlm.nih.gov/pubmed/27384425 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.orglett.6b01618 |
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