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Ring-expansion synthesis and crystal structure of dimethyl 4-ethyl-1,4,5,6,7,8-hexa­hydro­azonino[5,6-b]indole-2,3-di­carboxyl­ate

The title compound, C(20)H(24)N(2)O(4), is the product of a ring-expansion reaction from a seven-membered hexa­hydro­azepine to a nine-membered azonine. The azonine ring of the mol­ecule adopts a chair–boat conformation. In the crystal, mol­ecules are linked by bifurcated N—H⋯(O,O) hydrogen bonds, g...

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Detalhes bibliográficos
Publicado no:Acta Crystallogr E Crystallogr Commun
Main Authors: Nguyen, Van Tuyen, Sorokina, Elena A., Listratova, Anna V., Voskressensky, Leonid G., Lobanov, Nikolai N., Dorovatovskii, Pavel V., Zubavichus, Yan V., Khrustalev, Victor N.
Formato: Artigo
Idioma:Inglês
Publicado em: International Union of Crystallography 2017
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5347048/
https://ncbi.nlm.nih.gov/pubmed/28316803
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1107/S205698901700161X
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