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ITC-derived binding affinity may be biased due to titrant (nano)-aggregation. Binding of halogenated benzotriazoles to the catalytic domain of human protein kinase CK2

The binding of four bromobenzotriazoles to the catalytic subunit of human protein kinase CK2 was assessed by two complementary methods: Microscale Thermophoresis (MST) and Isothermal Titration Calorimetry (ITC). New algorithm proposed for the global analysis of MST pseudo-titration data enabled reli...

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Bibliographic Details
Published in:PLoS One
Main Authors: Winiewska, Maria, Bugajska, Ewa, Poznański, Jarosław
Format: Artigo
Language:Inglês
Published: Public Library of Science 2017
Subjects:
Online Access:https://ncbi.nlm.nih.gov/pmc/articles/PMC5342230/
https://ncbi.nlm.nih.gov/pubmed/28273138
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1371/journal.pone.0173260
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