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Trace Level Quantification of the (−)2-(2-amino-5-chlorophenyl)-4-cyclopropyl-1,1,1-trifluoro-3-butyn-2-ol Genotoxic Impurity in Efavirenz Drug Substance and Drug Product Using LC–MS/MS

Efavirenz is a non-nucleoside reverse transcriptase inhibitor used in the treatment of human immunodeficiency virus type-1 (HIV). (2S)-(2-Amino-5-chlorophenyl)-4-cyclopropyl-1,1,1-trifluoro-3-butyn-2-ol (AMCOL), used as an intermediate in the synthesis of efavirenz and a degradation impurity, has an...

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Publicado en:Sci Pharm
Autores principales: Jaishetty, Nagadeep, Palanisamy, Kamaraj, Maruthapillai, Arthanareeswari, Jaishetty, Rajamanohar
Formato: Artigo
Lenguaje:Inglês
Publicado: MDPI 2015
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Acceso en línea:https://ncbi.nlm.nih.gov/pmc/articles/PMC5064237/
https://ncbi.nlm.nih.gov/pubmed/28117312
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3390/scipharm84030456
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