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Rh-Catalyzed reductive Mannich-type reaction and its application towards the synthesis of (±)-ezetimibe

An effective synthesis for syn-β-lactams was achieved using a Rh-catalyzed reductive Mannich-type reaction. A rhodium–hydride complex (Rh–H) derived from diethylzinc (Et(2)Zn) and a Rh catalyst was used for the 1,4-reduction of an α,β-unsaturated ester to give a Reformatsky-type reagent, which in tu...

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Detalhes bibliográficos
Publicado no:Beilstein J Org Chem
Main Authors: Isoda, Motoyuki, Sato, Kazuyuki, Kunugi, Yurika, Tokonishi, Satsuki, Tarui, Atsushi, Omote, Masaaki, Minami, Hideki, Ando, Akira
Formato: Artigo
Idioma:Inglês
Publicado em: Beilstein-Institut 2016
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4979637/
https://ncbi.nlm.nih.gov/pubmed/27559413
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.12.157
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