Solid-State Dynamic Nuclear Polarization at 9.4 and 18.8 T from 100 K to Room Temperature

[Image: see text] Efficient dynamic nuclear polarization (DNP) in solids, which enables very high sensitivity NMR experiments, is currently limited to temperatures of around 100 K and below. Here we show how by choosing an adequate solvent, (1)H cross effect DNP enhancements of over 80 can be obtain...

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Pubblicato in:J Am Chem Soc
Autori principali: Lelli, Moreno, Chaudhari, Sachin R., Gajan, David, Casano, Gilles, Rossini, Aaron J., Ouari, Olivier, Tordo, Paul, Lesage, Anne, Emsley, Lyndon
Natura: Artigo
Lingua:Inglês
Pubblicazione: American Chemical Society 2015
Accesso online:https://ncbi.nlm.nih.gov/pmc/articles/PMC4671100/
https://ncbi.nlm.nih.gov/pubmed/26555676
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.5b08423
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