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Proton-detected 3D (1)H/(13)C/(1)H correlation experiment for structural analysis in rigid solids under ultrafast-MAS above 60 kHz

A proton-detected 3D (1)H/(13)C/(1)H chemical shift correlation experiment is proposed for the assignment of chemical shift resonances, identification of (13)C-(1)H connectivities, and proximities of (13)C-(1)H and (1)H-(1)H nuclei under ultrafast magic-angle-spinning (ultrafast-MAS) conditions. Ult...

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Vydáno v:J Chem Phys
Hlavní autoři: Zhang, Rongchun, Nishiyama, Yusuke, Ramamoorthy, Ayyalusamy
Médium: Artigo
Jazyk:Inglês
Vydáno: AIP Publishing LLC 2015
Témata:
On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC4617735/
https://ncbi.nlm.nih.gov/pubmed/26520504
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1063/1.4933373
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