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Crystal structures of 1,4-diazabicyclo[2.2.2]octan-1-ium 4-nitrobenzoate dihydrate and 1,4-diazabicyclo[2.2.2]octane-1,4-diium bis(4-nitrobenzoate): the influence of solvent upon the stoichiometry of the formed salt
The 1:1 co-crystallization of 1,4-diazabicyclo[2.2.2]octane (DABCO) with 4-nitrobenzoic acid in ethanol–water (3/1) gave the salt dihydrate C(6)H(13)N(2) (+)·C(7)H(4)NO(4) (−)·2H(2)O, (1), whereas from methanol, the salt C(6)H(14)N(2) (2+)·2C(7)H(4)NO(4) (−), (2), was isolated. In (1), the catio...
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| 主要な著者: | , , |
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| フォーマット: | Artigo |
| 言語: | Inglês |
| 出版事項: |
International Union of Crystallography
2014
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| 主題: | |
| オンライン･アクセス: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4120614/ https://ncbi.nlm.nih.gov/pubmed/25161500 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1107/S1600536814011532 |
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