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Multigramme synthesis and asymmetric dihydroxylation of a 4-fluorobut-2E-enoate
Esters of crotonic acid were brominated on a multigramme scale using a free radical procedure. A phase transfer catalysed fluorination transformed these species to the 4-fluorobut-2E-enoates reproducibly and at scale (48–53%, ca. 300 mmol). Asymmetric dihydroxylation reactions were then used to tran...
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| Main Authors: | , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
Beilstein-Institut
2013
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3869297/ https://ncbi.nlm.nih.gov/pubmed/24367430 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.9.301 |
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