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Total synthesis of peloruside A via kinetic lactonization and relay RCM cyclization reactions (and identification of iso-peloruside A)

A convergent total synthesis of peloruside A (1) is described. The key strategic features are a diastereoselective lactonization to generate a C5-C9 valerolactone from the C(2)-symmetric ketone 4, which comprises C1–C9 of 1, and a relay ring closing metathesis (RRCM) reaction to produce a dehydroval...

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Detalhes bibliográficos
Main Authors: Hoye, Thomas R., Jeon, Junha, Kopel, Lucas C., Ryba, Troy D., Tennakoon, Manomi A., Wang, Yini
Formato: Artigo
Idioma:Inglês
Publicado em: 2010
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3740187/
https://ncbi.nlm.nih.gov/pubmed/20645374
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201002293
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