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Dilute spin-exchange assignment of solid-state NMR spectra of oriented proteins: Acetylcholine M2 in bilayers

The assignment of amide resonances in the two-dimensional PISEMA (Polarization Inversion with Spin Exchange at the Magic Angle) spectrum of uniformly (15)N labeled M2 peptide corresponding to the channel-lining segment of the acetylcholine receptor in oriented phospholipid bilayers is described. The...

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Main Authors: Marassi, F.M., Gesell, J.J., Valente, A.P., Kim, Y., Oblatt-Montal, M., Montal, M., Opella, S.J.
Format: Artigo
Sprog:Inglês
Udgivet: 1999
Fag:
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC3282054/
https://ncbi.nlm.nih.gov/pubmed/10427741
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