A Comparison of NCO and NCA Transfer Methods for Biological Solid-State NMR Spectroscopy

Three different techniques (adiabatic passage Hartman-Hahn cross-polarization, optimal control designed pulses, and EXPORT) are compared for transferring (15)N magnetization to (13)C in solid-state NMR experiments under magic-angle-spinning conditions. We demonstrate that, in comparison to adiabatic...

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Bibliographic Details
Main Authors: Loening, Nikolaus M., Bjerring, Morten, Nielsen, Niels Chr., Oschkinat, Hartmut
Format: Artigo
Language:Inglês
Published: 2011
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Article
Online Access:https://ncbi.nlm.nih.gov/pmc/articles/PMC3257381/
https://ncbi.nlm.nih.gov/pubmed/22116035
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2011.10.012
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