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A Direct Comparison of Azide and Nitrile Vibrational Probes

The synthesis of 2′-azido-5-cyano-2′-deoxyuridine, N(3)CNdU (1), from trityl-protected 2′-amino-2′-deoxyuridine was accomplished in four steps with a 12.5% overall yield. The IR absorption positions and profiles of the azide and nitrile group of N(3)CNdU were investigated in 14 different solvents an...

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Autors principals: Gai, Xin Sonia, Coutifaris, Basil A., Brewer, Scott H., Fenlon, Edward E.
Format: Artigo
Idioma:Inglês
Publicat: 2011
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Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC3101501/
https://ncbi.nlm.nih.gov/pubmed/21336362
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c0cp02774j
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