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Two-dimensional concurrent HMQC-COSY as an approach for small molecule chemical shift assignment and compound identification

Chemical shift assignment is the first step toward the structure elucidation of natural products and other chemical compounds. We propose here the use of 2D concurrent HMQC-COSY as an experiment for rapid chemical shift assignment of small molecules. This experiment provides well-dispersed (1)H–(13)...

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Detalhes bibliográficos
Main Authors: Hu, Kaifeng, Westler, William M., Markley, John L.
Formato: Artigo
Idioma:Inglês
Publicado em: Springer Netherlands 2011
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3081433/
https://ncbi.nlm.nih.gov/pubmed/21373839
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-011-9494-4
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