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Hydrogen-Bond Detection, Configuration Assignment, and Rotamer Correction of Side-Chain Amides in Large Proteins by NMR through Protium/Deuterium Isotope Effects

In this study, the configuration and hydrogen-bonding network of side-chain amides in a 35 kDa protein are determined via measuring differential and across-hydrogen-bond H/D isotope effects by the IS-TROSY technique, which leads to a reliable recognition and correction of erroneous rotamers frequent...

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Detalhes bibliográficos
Main Authors: Liu, Aizhuo, Wang, Jifeng, Lu, Zhenwei, Yao, Lishan, Li, Yue, Yan, Honggao
Formato: Artigo
Idioma:Inglês
Publicado em: 2008
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3018730/
https://ncbi.nlm.nih.gov/pubmed/18973166
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/cbic.200800467
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