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Preparation and NMR spectra of four isomeric diformyl[2.2]paracyclophanes (cyclophanes 66)

Four isomeric dialdehydes 4, readily available from cycloaddition of propiolic aldehyde (2) to 1,2,4,5-hexatetraene (1), were separated by chromatography and recrystallization, and were characterized by their spectroscopic data. The individual isomers can now be easily identified from their (1)H NMR...

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Autori principali: Dix, Ina, Hopf, Henning, Satyanarayana, Thota B N, Ernst, Ludger
Natura: Artigo
Lingua:Inglês
Pubblicazione: Beilstein-Institut 2010
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Accesso online:https://ncbi.nlm.nih.gov/pmc/articles/PMC2981830/
https://ncbi.nlm.nih.gov/pubmed/21085510
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.6.104
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