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2-(Diphenylphosphinoylmethyl)pyrrole–2-(diphenylphosphinomethyl)pyrrole (0.43/0.57) and tetrachlorido(5-diphenylphosphinomethyl-2H-pyrrole-κ(2) N,P)titanium(IV)

The title phosphine oxide–phosphine, 0.43C(17)H(16)NOP·0.57C(17)H(16)NP, (I)/(II), was obtained as a 0.861 (6):1.139 (6) cocrystallized mixture. Hydrogen bonding between the two constituents leads to the formation of 2:2 solid-state assemblies. Instead of forming the expected simple N,P-chelated sys...

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Detalhes bibliográficos
Main Authors:	Broomfield, Lewis M., Bochmann, Manfred, Wright, Joseph A.
Formato:	Artigo
Idioma:	Inglês
Publicado em:	International Union of Crystallography 2010
Assuntos:	Metal-Organic Compounds
Acesso em linha:	https://ncbi.nlm.nih.gov/pmc/articles/PMC2855581/ https://ncbi.nlm.nih.gov/pubmed/20203400 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1107/S0108270110004506
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2-(Diphenyl­phosphinoylmeth­yl)pyrrole–2-(diphenyl­phosphinometh­yl)pyrrole (0.43/0.57) and tetra­chlorido­(5-diphenyl­phosphinometh­yl-2H-pyrrole-κ(2) N,P)titanium(IV)

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2-(Diphenylphosphinoylmethyl)pyrrole–2-(diphenylphosphinomethyl)pyrrole (0.43/0.57) and tetrachlorido(5-diphenylphosphinomethyl-2H-pyrrole-κ(2) N,P)titanium(IV)