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Synthesis of pyrrolo[1,3]diazepines by a dipolar cycloaddition – retro-Mannich domino reaction
Microwave irradiation facilitated the synthesis of 4-arylthio-3-oxazolin-5-ones from ethyl cyanoformate, thiophenol, and cyclic ketones. Subsequent decarboxylation and in situ [3+2] cycloaddition provided novel 2,3,4,5-tetrahydro-1H-pyrrolo[1,2-c][1,3]diazepine scaffolds after a spontaneous retro-Ma...
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| Main Authors: | , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2009
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2770875/ https://ncbi.nlm.nih.gov/pubmed/20160922 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2009.09.107 |
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