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Improved accuracy of (15)N-(1)H scalar and residual dipolar couplings from gradient-enhanced IPAP-HSQC experiments on protonated proteins
The presence of dipole-dipole cross-correlated relaxation as well as unresolved E.COSY effects adversely impacts the accuracy of (1)J(NH) splittings measured from gradient-enhanced IPAP-HSQC spectra. For isotropic samples, the size of the systematic errors caused by these effects depends on the valu...
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| Main Authors: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2009
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2753394/ https://ncbi.nlm.nih.gov/pubmed/19205898 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-009-9299-x |
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