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NMR Chemical Exchange as a Probe for Ligand-Binding Kinetics in a Theophylline-Binding RNA Aptamer

The apparent on- and off-rate constants for theophylline binding to its RNA aptamer in the absence of Mg(2+) were determined here by 2D (1)H-(1)H NMR ZZ-exchange spectroscopy. Analysis of the build-up rate of the exchange cross peaks for several base-paired imino protons in the RNA yielded an appare...

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Detalhes bibliográficos
Main Authors: Latham, Michael P., Zimmermann, Grant R., Pardi, Arthur
Formato: Artigo
Idioma:Inglês
Publicado em: 2009
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC2752443/
https://ncbi.nlm.nih.gov/pubmed/19317486
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja900695m
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