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Using Multiple Quantum Coherence to Increase the (15)N Resolution in a Three-Dimensional TROSY HNCO Experiment for Accurate PRE and RDC measurements
We present a new version of the 3D TROSY HNCO pulse scheme, referred to as HR-TROSY HNCO, with comparable resolution in the (15)N dimension to a 2D (1)H-(15)N HSQC experiment. In the conventional 3D TROSY HNCO, the constant time period (1/2J(NC′) ∼ 32 ms) severely limits the maximum resolution in th...
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| Main Authors: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2009
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2745499/ https://ncbi.nlm.nih.gov/pubmed/19615926 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2009.06.019 |
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