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Direct Measurements of Protein Backbone (15)N Spin Relaxation Rates from Peak Line-Width using a Fully-Relaxed Accordion 3D HNCO Experiment

Protein backbone (15)N spin relaxation rates measured by solution NMR provide useful dynamic information with a site-specific resolution. The conventional method is to record a series of 2D (1)H-(15)N HSQC spectra with varied relaxation delays, and derive relaxation rate from the following curve fit...

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Bibliographic Details
Main Authors: Chen, Kang, Tjandra, Nico
Format: Artigo
Language:Inglês
Published: 2008
Subjects:
Online Access:https://ncbi.nlm.nih.gov/pmc/articles/PMC2647993/
https://ncbi.nlm.nih.gov/pubmed/19114314
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2008.12.001
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