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Synthetic methodology for the preparation of N-hydroxysulfamides

A convenient synthesis of a variety of substituted N-hydroxysulfamides from chlorosulfonyl isocyanate is reported. Alkyl groups can be introduced selectively on the N-Boc nitrogen of key intermediates 1a or 1b using the Mitsunobu reaction with alcohols. Subsequently the nitrogen carrying the silylox...

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Hlavní autoři: Devanathan, Krishnaswamy, Bell, Jennifer A., Wilkins, Patricia C., Jacobs, Hollie K., Gopalan, Aravamudan S.
Médium: Artigo
Jazyk:Inglês
Vydáno: 2007
Témata:
On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC2330331/
https://ncbi.nlm.nih.gov/pubmed/18437247
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2007.09.037
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