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Class selection of amino acid metabolites in body fluids using chemical derivatization and their enhanced (13)C NMR
We report a chemical derivatization method that selects a class of metabolites from a complex mixture and enhances their detection by (13)C NMR. Acetylation of amines directly in aqueous medium with 1,1′-(13)C(2) acetic anhydride is a simple method that creates a high sensitivity and quantitative la...
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| Autors principals: | , , , , , |
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| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
National Academy of Sciences
2007
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC1913896/ https://ncbi.nlm.nih.gov/pubmed/17606902 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1073/pnas.0704449104 |
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