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Automated Microflow NMR: Routine Analysis of Five-Microliter Samples

A microflow CapNMR probe double-tuned for (1)H and (13)C was installed on a 400-MHz NMR spectrometer and interfaced to an automated liquid handler. Individual samples dissolved in DMSO-d(6) are submitted for NMR analysis in vials containing as little as 10 μL of sample. Sets of samples are submitted...

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Detalhes bibliográficos
Main Authors: Jansma, Ariane, Chuan, Tiffany, Geierstanger, Bernhard H., Albrecht, Robert W., Olson, Dean L., Peck, Timothy L.
Formato: Artigo
Idioma:Inglês
Publicado em: 2005
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Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC1395504/
https://ncbi.nlm.nih.gov/pubmed/16194121
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ac050936w
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