An expeditious and consistent procedure for tetrahydrofuran (THF) drying and deoxygenation by the still apparatus

Despite the availability of alternative methods for drying tetrahydrofuran (THF), the use of the still apparatus, wherein a THF solution containing Na-bezophenone ketyl is heated to reflux, remains widespread. We herein propose a set of procedures to solve the problems usually faced in applying this...

Disgrifiad llawn

Wedi'i Gadw mewn:
Manylion Llyfryddiaeth
Prif Awduron: Alessandro B. C. Simas, Vera L. P. Pereira, Cleber B. Barreto Jr., Daniel L. de Sales, Leandro L. de Carvalho
Fformat: Artigo
Iaith:Inglês
Cyhoeddwyd: Sociedade Brasileira de Química 2009-01-01
Cyfres:Química Nova
Pynciau:
THF
still apparatus
purification
Mynediad Ar-lein:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422009000900042
Tagiau: Ychwanegu Tag
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