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How to Clean and Safely Remove HF from Acid Digestion Solutions for Ultra-Trace Analysis: A Microwave-Assisted Vessel-Inside-Vessel Protocol

The complete dissolution of silicate-containing materials, often necessary for elemental determination, is generally performed by microwave-assisted digestion involving the forced use of hydrofluoric acid (HF). Although highly efficient in dissolving silicates, this acid exhibits many detrimental ef...

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Principais autores: Marco Pinna, Arianna Signorelli, Gilberto Binda, Carlo Dossi, Laura Rampazzi, Davide Spanu, Sandro Recchia
Format: Artigo
Sprog:Inglês
Udgivet: MDPI AG 2022-04-01
Serier:Methods and Protocols
Fag:
hydrofluoric acid
microwave-assisted acid digestion
soil
silicate dissolution
evaporation
ultra-trace elements
Online adgang:https://www.mdpi.com/2409-9279/5/2/30
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