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Development and Validation for Quantification of 7-Nitroso Impurity in Sitagliptin by Ultraperformance Liquid Chromatography with Triple Quadrupole Mass Spectrometry

The purpose of this research study was to develop an analytical method for the quantification of 7-nitroso-3-(trifluoromethyl)-5,6,7,8-tetrahydro-[1,2,4] triazolo [4,3-a] pyrazine (7-nitroso impurity), which is a potential genotoxic impurity. Since sitagliptin is an anti-diabetic medication used to...

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Principais autores: Hari Naga Prasada Reddy Chittireddy, J. V. Shanmukha Kumar, Anuradha Bhimireddy, Mohammed Rafi Shaik, Merajuddin Khan, Syed Farooq Adil, Mujeeb Khan, Fatimah N. Aldhuwayhi
Format: Artigo
Sprog:Inglês
Udgivet: MDPI AG 2022-12-01
Serier:Molecules
Fag:
sitagliptin
7-nitroso impurity
nitrosamine
UHPLC-MS/MS
ICH
Online adgang:https://www.mdpi.com/1420-3049/27/23/8581
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