Pentafluoropropionic Anhydride Derivatization and GC-MS Analysis of Histamine, Agmatine, Putrescine, and Spermidine: Effects of Solvents and Starting Column Temperature

Gas chromatography–mass spectrometry (GC-MS) is useful for the quantitative determination of the polyamines spermidine (SPD) and putrescine (PUT) and of the biogenic amine agmatine (AGM) in biological samples after derivatization. This GC-MS method involves a two-step extraction with <i>n</i>-butano...

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Principais autores:	Dimitrios Tsikas, Bibiana Beckmann, Svetlana Baskal, Gorig Brunner
Formato:	Artigo
Idioma:	Inglês
Publicado em:	MDPI AG 2023-01-01
coleção:	Molecules
Assuntos:	acylation amidation amines biogenic amines derivatization GC-MS
Acesso em linha:	https://www.mdpi.com/1420-3049/28/3/939
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