Solvent-free mechanochemical synthesis and X-ray studies of Cu(II) and Ni(II) complexes of 5-(3,4,5-Trimethoxybenzyl)pyrimidine-2,4-diamine (Trimethoprim) in a ball-mill
Solvent-free synthesis of [Cu(CH3COO)2(TMP)2](1) and [Ni(CH3COO)2(TMP)2](2) by ball milling of Cu(CH3COO)2.H2O and Ni(CH3COO)2.4H2O with Trimethoprim in the absence of solvent is described. Conventional synthesis of 1. CH3OH and 2. CH3OH was carried out by the reaction of metal acetate salt and Trim...
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| Principais autores: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
Springer
2016-09-01
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| coleção: | Journal of Saudi Chemical Society |
| Assuntos: | |
| Acesso em linha: | http://www.sciencedirect.com/science/article/pii/S1319610312002025 |
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